Inductively Coupled Plasma Mass Spectrometry
[NexION 2000, Perkin Elmer, USA]
Located at: CRF Annexe - S01
Facilities: ICP-MS-metal, Single cell and Single particle analysis, Microwave digestion system.
Applications: Environmental, Biological, Pharmaceutical, Petroleum, Food and Material testing samples.
Technical Specification for ICP-MS
1. Nebulizer type: Glass and PFA nebulizer.
2. Spray Chamber type: Glass and PFA spray chamber.
3. Maximum sample holding capacity of auto-sampler: 180.
4. Max TDS tolerance: > 25%
5. Minimum mass (within the mass range) of quadrupole in amu: 2
6. Maximum mass (within the mass range) of quadrupole in amu: 285
7. Minimum scan speed (amu/sec): 5000 amu/sec
8. Resolution (amu): 0.3
9. In-built or optional gas channels: 3
10. Gas channel for reactive inert and reactive gases: He, NH3, O2, CH4
11. Reaction Mode: Mass Shift
12. Type of Ion Detector: Electron multiplier
13. Sensitivity(mcps/ppm) Be(9): 6
14. Sensitivity(mcps/ppm) In(115): 100
15. Sensitivity(mcps/ppm) U(238): 80
16. Oxide ratio (%) CeO+/Ce+: ≤3
17. Doubly Charged Ratio (%) Ce++/Ce: <3
18. Background (CPS) measured at mass 220: ≤1
Microwave Digestion System
1. Minimum sample processing capacity in one batch: 15
2. Rated power of Microwave digestion system: 1500 Watt
3. Maximum operating temperature attained by microwave digestion system: 250oC
4. Maximum operating pressure attained by microwave digestion system: 40 bar
Sample Specification
1. Analysis of flowing elements are possible in ppm and ppb concentration range.
(Elements: Ag, Al, Au, Sb, As, B, Ba, Bi, Bo, Cd, Ca, Co, Cr, Cu, Fe, Ga, Ge, Hg, In, K, Li, Mg, Mn, Mo, Na, Ni, Pb, Rb, Sc, Se, Sr, Sn, Tb, Ti, V, Y, Zn)
2. Solid sample quantity: more than 0.5 grams
3. Liquid sample quantity: more than 2 ml
4. Rare earth elements and radioactive elements cannot be analysed
5. Pre-digested/prepared samples should not contain suspended particles
6. For interference free analysis, the samples must be digested with suprapure/trace-element grade acids
Testing charges
Details |
NITK |
Academic Institute* |
Industry* |
R&D Institute* |
Standardization [per element/sample] |
Rs. 250/- |
Rs. 750/- |
Rs. 2500/- |
Rs. 1500/- |
Measurement [Subsequent sample per element] |
Rs. 50/- |
Rs. 150/- |
Rs. 750/- |
Rs. 400/- |
Sample preparation [per sample] |
Rs. 500/- |
Rs. 1000/- |
Rs. 4000/- |
Rs. 2500/- |
*GST(18%) extra.
Above charges are for providing raw data.
For further Query Contact:
Ms. Thrithila Shetty (Technical Staff, CRF), Email: crf_icp@nitk.edu.in
Dr. I. Regupathi (ICP-MS Faculty in-charge), Email: regupathi@nitk.edu.in, Mob: +91-9731161327, Landline: 0824-2473609